I assume that you are referring to my article on Mail Merge to Email with
Attachments. If you have the path\filename of the file itself in the
catalog merge document, that is what should be attached. I use it several
times a day and it works perfectly for me (as long as the path\filename
details are one hundred percent correct so I always run a test where I
substitute my email address for each of the ones in the catalog to ensure
that I have everything OK.)
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Hope this helps,
Doug Robbins - Word MVP